Synthesis, crystal structure and vibrational spectra of a new diammonium zinc(II) dihydrogendiphosphate dihydrate, (NH4)2Zn(H 2P2O7)2·2H2O

Rachid Essehli, Mohammed Lachkar, Ingrid Svoboda, Hartmut Fuess, Brahim El Bali

Research output: Contribution to journalArticle

7 Citations (Scopus)

Abstract

The synthesis, crystal structure, and Raman study of the new dihydrogendiphosphate (NH4)2Zn(H2P 2O7) 2·2H2O, was reported. Three solutions were mixed in a beaker to prepare the compound, NH 4OH, ZnCl2·4H2O, and K4P 2O7. The Raman spectrum of the mentioned compound was measured in a back-scattering arrangment, under room conditions, using a high throughput holographic imaging filter and a thermoelectrically cooled CCD detector. It was observed that the longest hydrogen bonds occured between the hydroxyl species of the [H2P2O7] groups.

Original languageEnglish
JournalActa Crystallographica Section E: Structure Reports Online
Volume61
Issue number3
DOIs
Publication statusPublished - Mar 2005
Externally publishedYes

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Vibrational spectra
Charge coupled devices
Hydroxyl Radical
vibrational spectra
rooms
Raman scattering
Zinc
Hydrogen
charge coupled devices
Hydrogen bonds
zinc
Crystal structure
Throughput
Scattering
Raman spectra
hydrogen bonds
Detectors
Imaging techniques
filters
crystal structure

ASJC Scopus subject areas

  • Condensed Matter Physics
  • Structural Biology

Cite this

Synthesis, crystal structure and vibrational spectra of a new diammonium zinc(II) dihydrogendiphosphate dihydrate, (NH4)2Zn(H 2P2O7)2·2H2O. / Essehli, Rachid; Lachkar, Mohammed; Svoboda, Ingrid; Fuess, Hartmut; Bali, Brahim El.

In: Acta Crystallographica Section E: Structure Reports Online, Vol. 61, No. 3, 03.2005.

Research output: Contribution to journalArticle

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