Mesoporous PbO nanoparticle-catalyzed synthesis of arylbenzodioxy xanthenedione scaffolds under solvent-free conditions in a ball mill

Trimurti L. Lambat, Ratiram G. Chaudhary, Ahmed A. Abdala, Raghvendra Kumar Mishra, Sami H. Mahmood, Subhash Banerjee

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Abstract

A protocol for the efficient synthesis of arylbenzodioxy xanthenedione scaffolds was developed via a one-pot multi-component reaction of aromatic aldehydes, 2-hydroxy-1,4-naphthoquinone, and 3,4-methylenedioxy phenol using mesoporous PbO nanoparticles (NPs) as a catalyst under ball milling conditions. The synthesis protocol offers outstanding advantages, including short reaction time (60 min), excellent yields of the products (92-97%), solvent-free conditions, use of mild and reusable PbO NPs as a catalyst, simple purification of the products by recrystallization, and finally, the use of a green process of dry ball milling.

Original languageEnglish
Pages (from-to)31683-31690
Number of pages8
JournalRSC Advances
Volume9
Issue number54
DOIs
Publication statusPublished - 1 Jan 2019

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ASJC Scopus subject areas

  • Chemistry(all)
  • Chemical Engineering(all)

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